Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester → HCID 86589217, compound

HRID 1180066Notes

Reaction equation

HRID 1180066 reaction equation
O[CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11](=[O:20])[N:12]([CH3:19])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:6][CH:5]=1.[SH:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][N:23]=1>>[S:21]=[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][N:23]1[CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11](=[O:20])[N:12]([CH3:19])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 69520342Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl EsterHCID 178418616HCID 178418616, compound

Product 1

HCID 86589217HCID 86589217, compoundYield 25%

Procedure

The title compound was prepared in 25% yield as an oil using methyl-phenyl-carbamic acid 4-(2-hydroxy-ethyl)-phenyl ester and 2-mercaptopyridine. HPLC-MS: m/z=365.2 (M+1); Rt=4.08 min.

Sources & evidence

ORD record
ord-26468741db8a4d4286fdae6903ca2e59
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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