Methyl-phenyl-carbamic Acid 4-hydroxymethyl-phenyl Ester → HCID 86589218, compound

HRID 1180068Notes

Reaction equation

HRID 1180068 reaction equation
O[CH2:2][C:3]1[CH:8]=[CH:7][C:6]([O:9][C:10](=[O:19])[N:11]([CH3:18])[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:5][CH:4]=1.[SH:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][N:22]=1>>[S:20]=[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][N:22]1[CH2:2][C:3]1[CH:8]=[CH:7][C:6]([O:9][C:10](=[O:19])[N:11]([CH3:18])[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 69518671Methyl-phenyl-carbamic Acid 4-hydroxymethyl-phenyl EsterHCID 178418616HCID 178418616, compound

Product 1

HCID 86589218HCID 86589218, compoundYield 14%

Procedure

The title compound was prepared in 14% yield as an oil using methyl-phenyl-carbamic acid 4-hydroxymethyl-phenyl ester and 2-mercaptopyridine. HPLC-MS: m/z=351.1 (M+1); Rt=3.95 min.

Sources & evidence

ORD record
ord-236ddeb703774440abd55196dc139ec5
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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