HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester → HCID 69517908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester | HCID 69520342 | — |
| Reactant | HCID 178517760 | HCID 178517760 | — |
| Product | HCID 69517908 | HCID 69517908 | 24% |
Reaction Steps
The title compound was prepared in 24% yield as light yellow crystals using methyl-phenyl-carbamic acid 4-(2-hydroxy-ethyl)-phenyl ester and 2-hydroxypyrimidine. NMR (400 MHz; CDCl3): δ 3.11 (t, 2H), 3.42 (br s, 3H), 4.54 (t, 2H), 6.93 (t, 1H), 7.05 (d, 2H), 7.25-7.42 (m, 7H), 8.51 (d, 2H); HPLC-MS: m/z=350.2 (M+1); Rt=2.86 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279470B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-db926f741a814565be8ac1539a431af6 |
| Source note | uspto-grants-2007_10 |