HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-3-pyridinylamine → 2-(3-Methoxyphenyl)-N-{2-methoxy(5-pyridyl)}acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-3-pyridinylamine | HCID 81121 | — |
| Reactant | 3-Methoxyphenylacetyl chloride | HCID 2733246 | — |
| Product | 2-(3-Methoxyphenyl)-N-{2-methoxy(5-pyridyl)}acetamide | HCID 23440866 | 99% |
Reaction Steps
The title compound was prepared as described in Example 1. A, using 3-methoxyphenylacetyl chloride (4.8 g, 26.0 mmol) and 5-amino-2-methoxypyridine (3.23 g, 26.0 mmol) to afford the title compound (7.0 g, 99% yield): ES-MS (m/z) 272.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279489B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-6125f64dae9341fbb3e3bef2857967cf |
| Source note | uspto-grants-2007_10 |