HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 4-Methoxybenzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | Boron carbide | HCID 123279 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Methoxybenzophenone | HCID 69146 | 48.2% |
Reaction Steps
A mixture of 5.4 gm (0.05 moles) of anisole and 7.0 gm (0.05) moles of benzoyl chloride and 0.5 gm of boron carbide was placed in 50 ml of benzene. This mixture was allowed to react as described in Example 3. A yield of 48.2% of p-methoxy benzophenone was obtained, and 0.5 gm of the boron carbide catalysts was recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279604B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-1185fc3e6a64469d9b8dbfeb70c90873 |
| Source note | uspto-grants-2007_10 |