HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzaldehyde → HCID 42643333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 4-(tert-Butyldimethylsilyloxy)phenylboronic Acid (contains varying amounts of Anhydride) | HCID 11107815 | — |
| Product | HCID 42643333 | HCID 42643333 | — |
Reaction Steps
The title compound was prepared by reacting 4-bromobenzaldehyde (730 mg, 3.97 mmol) with 4-tert-butyl-dimethylsilyoxyphenylboronic acid (1.3 g, 5.16 mmol) according to Method B to yield 600 mg (48%) of white crystal: 1H NMR (DMSO-d6): δ 0.24 (6H, s), 1.01 (9H, s), 6.94 (2H, d, J=8.54 Hz), 7.53 (2H, d, J=8.56 Hz), 7.72 (2H, d, J=8.19 Hz), 7.93 (2H, d, 8.20 Hz), 10.04 (1H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279600B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-60714aa200f04a93a4834bbba94441c7 |
| Source note | uspto-grants-2007_10 |