HRID1180395

反应详情

EQUATION

反应方程式

HRID 1180395 的结构方程式

PROCEDURE

实验过程

Using the same protocol as described in example 23, step 2, (4-bromophenyl)(pyridin-3-yl)methanol from step 1 (644 mg, 2.4 mmol) was added to methyl 2-bromo-4-methylpentanoate (412 μL, 2.52 mmol). The crude residue was chromatographed on silica gel using 50% ethyl acetate in hexanes to afford the title compound.

WORKUP

后处理

  1. customThe crude residue was chromatographed on silica gel using 50% ethyl acetate in hexanes