HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-bromo-4-methylpentanoate → HCID 69472556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-bromo-4-methylpentanoate | HCID 12957039 | — |
| Reactant | (4-Bromophenyl)(thiazol-2-yl)methanol | HCID 14949088 | — |
| Product | HCID 69472556 | HCID 69472556 | — |
Reaction Steps
Using the same protocol as described in example 23, step 2, (4-bromophenyl)(1,3-thiazol-2-yl)methanol from step 1 (983 mg, 3.64 mmol) was added to methyl 2-bromo-4-methylpentanoate (624 μL, 3.82 mmol). The crude residue was chromatographed on silica gel using 25% ethyl acetate in hexanes to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279478B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-bfa3453ddb734985a328f0a4fafdaf5d |
| Source note | uspto-grants-2007_10 |