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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1180440Generated: November 1, 2026

Ethyl acetate hexane → HCID 86605404, compound

https://huagongshe.com/reaction/1180440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl acetate hexaneHCID 21226206—
Reactant(2S)-2-[(5-bromopyridin-2-yl)(phenyl)methoxy]-N-(cyanomethyl)-4-methylpentanamideHCID 86605403—
ProductHCID 86605404HCID 86605404—

Reaction Steps

Using the same procedure as described for example 40, (2S)-2-[(5-bromopyridin-2-yl)(phenyl)methoxy]-N-(cyanomethyl)-4-methylpentanamide (51 mg, 0.123 mmol) was oxidized to give the title compound after chromatography with 50% EtOAc/hexane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07279478B2
Source datasetuspto-grants-2007_10
ORD IDord-5208ac0e1ccb47008538730cf2a928fc
Source noteuspto-grants-2007_10