HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Ethanedithiol → HCID 131726112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Ethanedithiol | HCID 10902 | — |
| Reactant | HCID 131726110 | HCID 131726110 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131726112 | HCID 131726112 | — |
Reaction Steps
1,2-Ethanedithiol (Aldrich; 25 μl, 0.30 mmol) was added to 4-(bromopropionamido)-phenylarsineoxide as prepared above(100 mg, 0.30 mol) dissolved in 1 ml of hot methanol. After 5 min, a white solid precipitated and was collected. Yield: 63.7 mg, 0.16 mmol, 53%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07282373B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-0c8c5535813047fead5d359345089059 |
| Source note | uspto-grants-2007_10 |