2-Bromo-9H-fluorene → HCID 58978752, compound
Reaction equation
Br[CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8].[Br:9][C:10]1[CH:22]=[CH:21][C:20]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH2:13][C:12]=2[CH:11]=1>>[Br:9][C:10]1[CH:22]=[CH:21][C:20]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[C:13]([CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8])([CH2:2][CH2:3][O:4][CH2:5][CH2:6][O:7][CH3:8])[C:12]=2[CH:11]=1Participants
3
Procedure
2-Bromo-9,9-bis(3,6-dioxaheptyl)-fluorene (14) was synthesized from bromo-2-(2-methoxyethoxy)ethane and 2-bromofluorene following the general procedure outlined in Example 3.
Sources & evidence
- ORD record
- ord-68a14eae657a44efa7c75eab29963203
- Source dataset
- uspto-grants-2007_10
- Patent number
- US07282275B2
Reaction notes
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