HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → p-Toluenesulfonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | p-Toluenesulfonic acid | HCID 6101 | 239.9% |
Reaction Steps
To this solution, 40 ml of toluene was added, and then 11.27 g (59.3 mmol, 1.0 eq) of p-toluenesulfonic acid monohydrate was added and dissolved under heating. Then, the solution was cooled to crystallize, thereby obtaining 24.5 g (yield: 85%) of p-toluene sulfonic acid (PTS) salt of Exemplified compound (21).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07282610B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-72a0396d493144d2b91832ee55b55516 |
| Source note | uspto-grants-2007_10 |