HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylhydrazine monohydrochloride → 1-tert-butyl-3-(4-nitrophenyl)-1H-pyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylhydrazine monohydrochloride | HCID 81889 | — |
| Reactant | HCID 69001014 | HCID 69001014 | — |
| Product | 1-tert-butyl-3-(4-nitrophenyl)-1H-pyrazole | HCID 53485528 | — |
Reaction Steps
Following the procedure described for Intermediate 1 with t-butylhydrazine hydrochloride, provided the title compound as the minor isomer. ESMS (M−C(CH3)3+2H): 190.0; HNMR (400 MHz, d6-DMSO)8.20 (d, 2H), 7.86 (d, 2H), 7.7(d, 1H), 6.55(d, 1H), 1.25 (s, 9H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07282588B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-ae0323dd21a246e9abe16cce46e56390 |
| Source note | uspto-grants-2007_10 |