Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aluminium lithium hydride → N9-phenethyl-8-hydroxymethyladenine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 반응물 | N9-phenethyl-8-methoxycarbonyladenine | HCID 42637713 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N9-phenethyl-8-hydroxymethyladenine | HCID 42637018 | — |
반응 단계
A solution of N9-phenethyl-8-methoxycarbonyladenine (1 mmol) in tetrahydrofuran was treated with lithium aluminum hydride (1 mmol) at 0° C. for 1 h. Extraction and chromatography gave N9-phenethyl-8-hydroxymethyl-adenine as a white solid. TLC: Rf=0.31, 10% MeOH—CH2Cl2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07285543B2 |
| 출처 데이터셋 | uspto-grants-2007_10 |
| ORD ID | ord-ca59b78df4b54ff7aae5624bb505f4b7 |
| 출처 메모 | uspto-grants-2007_10 |