HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,6-Dichloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidine → HCID 86606975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,6-Dichloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidine | HCID 21979566 | — |
| Reactant | Benzylsulfamic acid amide potassium salt | HCID 68727905 | — |
| Product | HCID 86606975 | HCID 86606975 | 47% |
Reaction Steps
Benzylsulfamic acid [6-chloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidinyl]-amide (0.7 g) was prepared from 4,6-dichloro-5-(2-chloro-5-methoxy-phenoxy)-pyrimidine (1 g) and benzylsulfamic acid amide potassium salt (1.21 g) according to the procedure described in Referential Example 15. LC-MS: tR=5.13; [M+H]+=456.91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07285549B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-cdc90716dfd8448091cf80e17306cc2d |
| Source note | uspto-grants-2007_10 |