HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1181371Generated: November 1, 2026
1-Pyrrolidineethanamine → HCID 58980897, compound
https://huagongshe.com/reaction/1181371
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Pyrrolidineethanamine | HCID 1344 | — |
| Reactant | 2-Chloro-5-nitroanisole | HCID 70519 | — |
| Product | HCID 58980897 | HCID 58980897 | 24% |
Reaction Steps
A neat mixture of 1-chloro-2-methoxy-4-nitrobenzene (2.0 g, 10.7 mmol) and 2-pyrrolidin-1-ylethanamine (2.5 g, 22 mmol) was heated to 75° C. overnight, then chromatographed on silica gel with ethanol (100%) to give a yellow solid (0.67 g, 24%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07285557B2 |
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| Source dataset | uspto-grants-2007_10 |
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| ORD ID | ord-4add254f56fb412e8df17e37fc794b74 |
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| Source note | uspto-grants-2007_10 |
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