1-Benzothiophene-3-carbaldehyde → HCID 58980988, compound

HRID 1181693Notes

Reaction equation

HRID 1181693 reaction equation
[NH:1]([C:3]1[N:8]([CH2:9][CH:10]([CH3:12])[CH3:11])[C:7](=[O:13])[N:6]([CH3:14])[C:5](=[O:15])[CH:4]=1)[NH2:2].[S:16]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[C:18]([CH:25]=O)=[CH:17]1.[CH:27]([C:29]1[N:33]([CH3:34])[CH:32]=[C:31]([C:35]([O:37][CH3:38])=[O:36])[CH:30]=1)=O>>[S:16]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[C:18]([CH2:25][N:2]2[C:27]([C:29]3[N:33]([CH3:34])[CH:32]=[C:31]([C:35]([O:37][CH3:38])=[O:36])[CH:30]=3)=[C:4]3[C:3]([N:8]([CH2:9][CH:10]([CH3:11])[CH3:12])[C:7](=[O:13])[N:6]([CH3:14])[C:5]3=[O:15])=[N:1]2)=[CH:17]1

Participants

4

Reactant 3

HCID 2273281-Benzothiophene-3-carbaldehydeHCID 14173855methyl 5-formyl-1-methyl-1H-pyrrole-3-carboxylateHCID 193560846-hydrazino-1-isobutyl-3-methyl-2,4(1H,3H)-pyrimidinedione

Product 1

HCID 58980988HCID 58980988, compound

Procedure

This compound was made following the procedure described above, starting with 6-hydrazino-1-isobutyl-3-methylpyrimidine-2,4(1H,3H)-dione, and condensing first with 1-benzothiophene-3-carbaldehyde, followed by methyl 5-formyl-1-methyl-1H-pyrrole-3-carboxylate. Mass: 506.31 (M+H).

Sources & evidence

ORD record
ord-c4e0f30ed06f4662aad3ebbbb7d44c77
Source dataset
uspto-grants-2007_10
Patent number
US07285558B2

Reaction notes

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