1-Methyl-2-imidazolecarboxaldehyde → HCID 58981005, compound

HRID 1181829Notes

Reaction equation

HRID 1181829 reaction equation
[NH:1]([C:3]1[N:8]([CH2:9][CH:10]([CH3:12])[CH3:11])[C:7](=[O:13])[N:6]([CH3:14])[C:5](=[O:15])[CH:4]=1)[NH2:2].[S:16]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[C:18]([CH:25]=O)=[CH:17]1.[CH3:27][N:28]1[CH:32]=[CH:31][N:30]=[C:29]1[CH:33]=O>>[S:16]1[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=2[C:18]([CH2:25][N:2]2[C:33]([C:29]3[N:28]([CH3:27])[CH:32]=[CH:31][N:30]=3)=[C:4]3[C:3]([N:8]([CH2:9][CH:10]([CH3:11])[CH3:12])[C:7](=[O:13])[N:6]([CH3:14])[C:5]3=[O:15])=[N:1]2)=[CH:17]1

Participants

4

Reactant 3

HCID 1395751-Methyl-2-imidazolecarboxaldehydeHCID 2273281-Benzothiophene-3-carbaldehydeHCID 193560846-hydrazino-1-isobutyl-3-methyl-2,4(1H,3H)-pyrimidinedione

Product 1

HCID 58981005HCID 58981005, compound

Procedure

This compound was made following the procedure described above, starting with 6-hydrazino-1-isobutyl-3-methylpyrimidine-2,4(1H,3H)-dione, and condensing first with 1-benzothiophene-3-carbaldehyde, followed by 1-methyl-1H-imidazole-2-carbaldehyde. 448.5 (M+H).

Sources & evidence

ORD record
ord-3f6f0f243bf4499f9ee10d6a27ceee49
Source dataset
uspto-grants-2007_10
Patent number
US07285558B2

Reaction notes

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