2-Phenylethanol → HCID 22253141, compound

HRID 1182000Notes

Reaction equation

HRID 1182000 reaction equation
[C:1]1([CH2:7][CH2:8][OH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:10].[NH2:11][CH2:12][C:13](=[O:19])[CH2:14][CH2:15][C:16](O)=[O:17]>>[ClH:10].[NH2:11][CH2:12][C:13](=[O:19])[CH2:14][CH2:15][C:16]([O:9][CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:17]

Participants

3

Reactant 2

HCID 60542-PhenylethanolHCID 123608Aminolevulinic Acid Hydrochloride

Product 1

HCID 22253141HCID 22253141, compound

Procedure

From 2-phenylethanol (5.0 g; 41 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 70° C. The reaction was complete after 3 h. The yield was 1.43 g (88%).

Workup

  1. customat 70° C

Sources & evidence

ORD record
ord-b03680524d99481c8a9d6b14c973b304
Source dataset
uspto-grants-2007_10
Patent number
US07287646B2

Reaction notes

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