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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1182245Generated: November 1, 2026

Isopropanol → HCID 69424771, compound

https://huagongshe.com/reaction/1182245

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsopropanolHCID 3776—
ReactantEthyl AcetateHCID 8857—
ReactantPotassium hydroxy sulfiteHCID 23707502—
ReactantHCID 69423988HCID 69423988—
SolventWaterHCID 962—
ProductHCID 69424771HCID 69424771—

Reaction Steps

A solution of 5-(3-benzyloxycarbonylamino-2-oxo-pyrrolidin-1-yl)-4-isopropylsulfanylmethyloctahydro-cyclopenta[c]pyrrole-2-carboxylic acid tert-butyl ester in isopropanol is treated with a solution of oxone in water. The reaction mixture is stirred at room temperature until the reaction is complete, and then water and ethyl acetate are added. The organic layer is separated, dried over sodium sulfate and concentrated under vacuum providing the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07288563B2
Source datasetuspto-grants-2007_10
ORD IDord-e944bd5af02f460dafaccce2b2db6718
Source noteuspto-grants-2007_10