2-Aminophenol → HCID 58982136, compound

Participants

Reaction Steps

Following the procedure described in Example 22, but substituting carboxylic acid 50h for carboxylic acid 50g and 2-aminophenol for 1,2-phenylenediamine, the title compound 74 was obtained in 39% yield. 1H NMR (CDCl3:CD3OD 5:1): δ 7.99 (d, J=8.4 Hz, 2H), 7.60 (m, 4H), 7.41 (m, 4H), 7.02 (m, 1H), 6.91 (m, 1H), 6.81 (m, 1H), 2.98 (m, 2H), 2.41 (t, J=7.5 Hz, 2H), 1.74 (m, 4H), 1.42 (m, 4H).

Provenance & Evidence