HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 49764311, compound → HCID 49764433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 49764311 | HCID 49764311 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 49764433 | HCID 49764433 | 33.8% |
Reaction Steps
A suspension of Example 19 (53 mg) and Pd/C (10%, 62 mg) in MeOH (2 mL) was stirred at RT under H2 atmosphere until reaction completion. The reaction mixture was filtrated over celite and the filtrate evaporated to dryness. Preparative HPLC (I) gave 18 mg of the desired product as yellow foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664203B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-be0401f095054d06816e3dd8a7157f51 |
| Source note | uspto-grants-2014_03 |