Aluminium lithium hydride → HCID 67434598, compound

HRID 1182702Notes

Reaction equation

HRID 1182702 reaction equation
[CH2:1]([NH:8][C:9]1[C:14]([C:15](O)=[O:16])=[CH:13][N:12]=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[CH2:1]([NH:8][C:9]1[CH:10]=[CH:11][N:12]=[CH:13][C:14]=1[CH2:15][OH:16])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 67434626HCID 67434626, compound

Product 1

HCID 67434598HCID 67434598, compound

Procedure

Starting from 4-(benzylamino)nicotinic acid using 4 eq of LiAlH4 yielded the title compound. ESI-MS [M+H]+=215.1.

Sources & evidence

ORD record
ord-3e63dab9efa049fd84520575c4ab2dcc
Source dataset
uspto-grants-2014_03
Patent number
US08664214B2

Reaction notes

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