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HRID1182868

反应详情

EQUATION

反应方程式

HRID 1182868 的结构方程式

REACTANTS

反应物

2
结构：Cl.Cl.NO[C@@H]1CCNC1
HCID66713918

未命名化合物

结构：CC[C@H]1C(=O)CC[C@@]2(C)C1[C@@H](O)C[C@@H]1[C@@H]2CC[C@]2(C)C(=O)CC[C@@H]12
HCID68731819

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@H]1/C(=N/O[C@@H]2CCNC2)CC[C@@]2(C)C1[C@@H](O)C[C@@H]1[C@@H]2CC[C@]2(C)C(=O)CC[C@@H]12.Cl
HCID87571573

未命名化合物

PROCEDURE

实验过程

The title compound was obtained in 90% yield following the procedure described in Example 30 starting from 4β-ethyl-6α-hydroxyandrostan-3,17-dione (Preparation 27, 137 mg) and 3-(R)-pyrrolidinyloxyamine dihydrochloride (Preparation 12, 160 mg). The crude product was triturated with Et2O and the resulting precipitate was filtered to give the title compound I-bx.

WORKUP

后处理

  1. customThe crude product was triturated with Et2O
  2. filtrationthe resulting precipitate was filtered