Benzophenone oxime → Benzophenone O-(3-methylamino-propyl)oxime

HRID 1182883Notes

Reaction equation

HRID 1182883 reaction equation
[C:1](=[N:14][OH:15])([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl.[CH3:17][NH:18][CH2:19][CH2:20][CH2:21]Cl>>[CH3:17][NH:18][CH2:19][CH2:20][CH2:21][O:15][N:14]=[C:1]([C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 11324Benzophenone oximeHCID 22107021(3-Chloropropyl)(methyl)amine hydrochloride

Product 1

HCID 86649202Benzophenone O-(3-methylamino-propyl)oximeYield 62%

Procedure

Benzophenone O-(3-methylamino-propyl)oxime was prepared in 62% yield from benzophenone oxime and N-methyl-3-chloropropylamine hydrochloride by the procedure described above for the preparation of benzophenone O-(2-N-methylaminoethyl)oxime (Preparation 13, Step 1).

Sources & evidence

ORD record
ord-89823f77db3c43fe9c62b1b63812d738
Source dataset
uspto-grants-2014_03
Patent number
US08664210B2

Reaction notes

Loading…