Sodium Bicarbonate → HCID 68749371, compound

Participants

Reaction Conditions

Reaction Steps

The product of Example 1 (2.1 g) was mixed with 10% TFA/DCM (50 ml) and stirred at 0° C. for 2 hours. Saturated NaHCO3 (80 ml) was added to the solution at 0° C. and the solution was further extracted with EtOAc twice. The combined organic layer was washed with water, brine and dried over Na2SO4. The solution was evaporated to give the titled compound for next step without further purification. Mass: (M+1), 575

Provenance & Evidence