Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dibenzofuran | HCID 568 | — |
| Reactant | Iodine | HCID 807 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Orthoperiodic acid | HCID 25289 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Iododibenzofuran | HCID 223327 | — |
Reaction Steps
In a 500 mL three-neck flask was put a suspension of 8.4 g (50 mmol) of dibenzofuran, 6.2 g (25 mmol) of iodine, 5.7 g (25 mmol) of orthoperiodic acid, 150 mL of glacial acetic acid, 30 mL of water, and 500 μL of sulfuric acid, and the suspension was heated and stirred at 60° C. for 4.5 hours to cause a reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08664263B2 |
|---|
| Source dataset | uspto-grants-2014_03 |
|---|
| ORD ID | ord-b9923b8b10374364ba78da49e7cf6de8 |
|---|
| Source note | uspto-grants-2014_03 |
|---|
