HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 1-Benzoyl-1,3-dicyclohexyl-O-(N-2-butylideneamino)-isourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,3-Dicyclohexyl-O-(N-2-butylideneamino)-isourea | HCID 86664633 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 1-Benzoyl-1,3-dicyclohexyl-O-(N-2-butylideneamino)-isourea | HCID 86664640 | 72.4% |
Reaction Steps
To a solution of 1,3-dicyclohexyl-O—(N-2-butylideneamino)-isourea (Cmpd. 2) (7.34 g, 25 mmol) and 4-dimethylaminopyridine (100 mg) in dichloromethane (25 ml) and triethylamine (3.9 ml, 27.5 mmol) is added benzoyl chloride (3.58 g, 25.5 mmol). The mixture is stirred 6 h at room temperature, diluted with hexane (200 ml), washed with water (4×20 ml), dried over MgSO4 and evaporated. The residue is chromatographed on silica gel (hexanes-ethyl acetate 4:1) and the pure fractions are recrystallized from hexane to afford 7.2 g of the title compound as white crystals, mp 74-78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664288B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-21e258fb824b4ce59a7c7ef969cdaf7f |
| Source note | uspto-grants-2014_03 |