Phenylacetyl chloride → HCID 66577754, compound

HRID 1183303Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[C:14]([NH:16][NH2:17])=[O:15])=[CH:4][CH:3]=1.[C:18]1([CH2:24][C:25](Cl)=O)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[CH2:24]([C:25]1[O:15][C:14]([C:9]2[C:10]([CH3:13])=[N:11][O:12][C:8]=2[C:5]2[CH:6]=[CH:7][C:2]([Br:1])=[CH:3][CH:4]=2)=[N:16][N:17]=1)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

Reactant 2

HCID 7679Phenylacetyl chloride

HCID 66577662HCID 66577662, compound

Product 1

HCID 66577754HCID 66577754, compound

Procedure

Prepared according to the procedure described in Example 8, Step 6, using 5-(4-bromo-phenyl)-3-methyl-isoxazole-4-carboxylic acid hydrazide and phenylacetyl chloride.

Workup

customPrepared

Sources & evidence

ORD record: ord-f3c2116d9ecb47d7b204bc30dac86ebe
Source dataset: uspto-grants-2014_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08664220B2

Reaction notes

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