Benzyl azide → HCID 66579383, compound

HRID 1183359Notes

Reaction equation

HRID 1183359 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[CH:14]([NH:17][S:18]([CH3:21])(=[O:20])=[O:19])[C:15]#[CH:16])=[CH:4][CH:3]=1.[CH2:22]([N:29]=[N+:30]=[N-:31])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[CH2:22]([N:29]1[CH:16]=[C:15]([CH:14]([C:9]2[C:10]([CH3:13])=[N:11][O:12][C:8]=2[C:5]2[CH:4]=[CH:3][C:2]([Br:1])=[CH:7][CH:6]=2)[NH:17][S:18]([CH3:21])(=[O:20])=[O:19])[N:31]=[N:30]1)[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 12152Benzyl azideHCID 86679092HCID 86679092, compound

Product 1

HCID 66579383HCID 66579383, compound

Procedure

Prepared according to the procedure described in Example 40, Step 2, using N-{1-[5-(4-bromo-phenyl)-3-methyl-isoxazol-4-yl]-prop-2-ynyl}-methanesulfonamide and benzyl azide.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-5dc5081b932d40be8f5ea1edfdce45dd
Source dataset
uspto-grants-2014_03
Patent number
US08664220B2

Reaction notes

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