Tributyltin azide → HCID 66577851, compound

Participants

Reaction Conditions

Reaction Steps

1-{4′-[4-(6-Cyano-pyridin-2-ylamino)-3-methyl-isoxazol-5-yl]-biphenyl-4-yl}-cyclopropanecarboxylic acid ethyl ester (0.046 g, 0.1 mmol) and azidotributyltin(IV) (0.0996 g, 0.3 mmol) were dissolved in dichlorobenzene (1 mL) and heated to 110° C. for 14 hours. After cooling the reaction mixture was directly purified by silica gel chromatography to afford the title compound.

Provenance & Evidence