HuagongsheHuagongshe Chemistry Print Report · For research reference only
Titanium tetrabutoxide → HCID 86657295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Titanium tetrabutoxide | HCID 21801 | — |
| Reactant | HCID 86657296 | HCID 86657296 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86657295 | HCID 86657295 | 196.9% |
Reaction Steps
177 g (1 mol) of methyl 3-(ethylhydroxyphosphinyl)-2-methylpropionate (produced as in Example 6) and 140 g of titanium tetrabutoxide are refluxed in 500 ml of toluene for 40 hours. The resulting butanol is distilled off from time to time with proportions of toluene. The solution formed is subsequently freed of solvent to leave 196 g of methyl 3-(ethylhydroxyphosphinyl)-2-methylpropionate titanium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08664418B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-5550ebc5f61f48678b29778284643073 |
| Source note | uspto-grants-2014_03 |