HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 86680538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 2,2-Difluoroethanamine | HCID 136274 | — |
| Reactant | HCID 86680539 | HCID 86680539 | — |
| Product | HCID 86680538 | HCID 86680538 | — |
Reaction Steps
The title compound was prepared as a trifluoroacetic acid salt according to the procedure described in Example 194B, substituting the product from Example 179A for the product from Example 194A, and substituting 2,2-difluoroethanamine for ethylamine. 1H NMR (300 MHz, CDCl3) δ ppm 0.89-1.07 (m, 4 H) 7.52-7.66 (m, 3 H) 7.67-7.80 (m, 1 H) 7.87-7.97 (m, 1 H) 7.97-8.12 (m, 1 H); MS (ESI) m/z 526 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669255B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-d7999aa46e194bd5bfb505a062771fd3 |
| Source note | uspto-grants-2014_03 |