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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1184620Generated: November 3, 2026

Ethylamine → HCID 86680538, compound

https://huagongshe.com/reaction/1184620

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylamineHCID 6341—
ReactantTrifluoroacetic acidHCID 6422—
Reactant2,2-DifluoroethanamineHCID 136274—
ReactantHCID 86680539HCID 86680539—
ProductHCID 86680538HCID 86680538—

Reaction Steps

The title compound was prepared as a trifluoroacetic acid salt according to the procedure described in Example 194B, substituting the product from Example 179A for the product from Example 194A, and substituting 2,2-difluoroethanamine for ethylamine. 1H NMR (300 MHz, CDCl3) δ ppm 0.89-1.07 (m, 4 H) 7.52-7.66 (m, 3 H) 7.67-7.80 (m, 1 H) 7.87-7.97 (m, 1 H) 7.97-8.12 (m, 1 H); MS (ESI) m/z 526 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08669255B2
Source datasetuspto-grants-2014_03
ORD IDord-d7999aa46e194bd5bfb505a062771fd3
Source noteuspto-grants-2014_03