HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 86680540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 3,3-Difluoropyrrolidine | HCID 2782827 | — |
| Reactant | HCID 86680539 | HCID 86680539 | — |
| Product | HCID 86680540 | HCID 86680540 | — |
Reaction Steps
The title compound was prepared as a trifluoroacetic acid salt according to the procedure described in Example 194B, substituting the product from Example 179A for the product from Example 194A, and substituting 3,3-difluoropyrrolidine for ethylamine. 1H NMR (300 MHz, CDCl3) δ ppm 0.88-1.07 (m, 4 H) 5.37-5.59 (m, 2 H) 7.57-7.73 (m, 3 H) 7.75-7.87 (m, 1 H) 7.89-7.96 (m, 1 H) 7.98-8.12 (m, 1 H); MS (ESI) m/z 552 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669255B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-0da7226ab27841bba6085119690d4ed3 |
| Source note | uspto-grants-2014_03 |