HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-4-methylpyridine-3-boronic acid → HCID 86674891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-4-methylpyridine-3-boronic acid | HCID 44119169 | — |
| Reactant | 4-(5-Bromo-2,3-dihydro-benzofuran-2-yl)-piperidine-1-carboxylic acid isopropyl ester | HCID 67973262 | — |
| Product | HCID 86674891 | HCID 86674891 | — |
Reaction Steps
The title compound is prepared from 4-(5-bromo-2,3-dihydro-benzofuran-2-yl)-piperidine-1-carboxylic acid isopropyl ester and 2-chloro-4-methylpyridine-5-boronic acid following a procedure analogous to that described for Intermediate 15. LC (method 6): tR=1.40 min; Mass spectrum (ESI+): m/z=415 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669271B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-671eb2eebe844e679d5c0c9b59178949 |
| Source note | uspto-grants-2014_03 |