HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile, 4-bromo- → HCID 57389142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile, 4-bromo- | HCID 12162 | — |
| Reactant | HCID 67973765 | HCID 67973765 | — |
| Product | HCID 57389142 | HCID 57389142 | 66% |
Reaction Steps
The title compound is prepared from 4-[5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-2,3-dihydro-benzofuran-2-yl]-piperidine-1-carboxylic acid isopropyl ester and 4-bromo-benzonitrile following a procedure analogous to that described in Example 1. Yield: 66% of theory; LC (method 1): tR=1.52 min; Mass spectrum (ESI+): m/z=391 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669271B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-5f9f7bead2b346d49f30292c79f315e8 |
| Source note | uspto-grants-2014_03 |