HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-((Methylamino)sulphonyl)benzene boronic acid → HCID 67990261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-((Methylamino)sulphonyl)benzene boronic acid | HCID 44118763 | — |
| Reactant | 4-(5-Chloro-2,3-dihydrofuro[2,3-c]pyridin-2-yl)piperidine-1-carboxylic acid tert-butyl ester | HCID 86674895 | — |
| Product | HCID 67990261 | HCID 67990261 | — |
Reaction Steps
The title compound is prepared from 4-(5-chloro-2,3-dihydro-furo[2,3-c]pyridin-2-yl)-piperidine-1-carboxylic acid tert-butyl ester and 4-(methylaminosulfonyl)phenylboronic acid acid following a procedure analogous to that described in Example 28. LC (method 7): tR=1.33 min; Mass spectrum (ESI+): m/z=474 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669271B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-483e51362a0d4837b9ac1d9b24f256a6 |
| Source note | uspto-grants-2014_03 |