HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl chloroformate → HCID 71115001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl chloroformate | HCID 7917 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 67973724 | HCID 67973724 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71115001 | HCID 71115001 | — |
Reaction Steps
The title compound is prepared from (S)-5-(1-methanesulfonyl-1,2,3,6-tetrahydro-pyridin-4-yl)-2-methyl-2-piperidin-4-yl-2,3-dihydro-furo[2,3-c]pyridine by treatment with isopropyl chloroformate in the presence of triethylamine using dichloromethane as a solvent. LC (method 6): tR=0.96 min; Mass spectrum (ESI+): m/z=464 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669271B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-c94ac15738104209873ffa0dff9065bf |
| Source note | uspto-grants-2014_03 |