HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Methylsulfonyl)piperazine → HCID 67990263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Methylsulfonyl)piperazine | HCID 709161 | — |
| Reactant | 4-(5-Chloro-2,3-dihydrofuro[2,3-c]pyridin-2-yl)piperidine-1-carboxylic acid tert-butyl ester | HCID 86674895 | — |
| Product | HCID 67990263 | HCID 67990263 | — |
Reaction Steps
The title compound is prepared from 4-(5-chloro-2,3-dihydro-furo[2,3-c]pyridin-2-yl)-piperidine-1-carboxylic acid tert-butyl ester and 1-(methylsulfonyl)piperazine following a procedure analogous to that described in Example 79. LC (method 10): tR=1.41 min; Mass spectrum (ESI+): m/z=467 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669271B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-211615d60edb434dbe91e242dc21ad72 |
| Source note | uspto-grants-2014_03 |