3,3'-(1,1,3,3-Tetramethyldisiloxane-1,3-diyl)bispropylamine → Tetramethylammonium 3-aminopropyldimethylsilanolate

Participants

Reaction Steps

A 250 ml three-neck round-bottom flask equipped with a magnetic stirrer, argon inlet, and condenser with drying tube was charged with 12.4 g (0.05 mol) of 1,3-bis(3-aminopropyl)tetramethyldisiloxane, 18.1 (88.12 mmol) of tetramethylammonium hydroxide pentahydrate, and 30 ml of tetrahydrofuran. The mixture was heated under reflux in an inert gas atmosphere for 5 hours.

Provenance & Evidence