Dicyclohexylcarbodiimide → HCID 58526175, compound

Participants

Reaction Steps

To a solution of dicyclohexylcarbodiimide (10.3 g, 50 mmol) and N,N-diethylhydroxylamine (6.7 g, 75 mmol) in THF (30 ml) is added finely powdered NaOH (0.2 g) and the mixture is stirred at room temperature for 50 hours. The reaction mixture is then filtered and the filtrate is evaporated on the rotary evaporator below 45° C. to afford 13.24 g of the title compound as a light yellow oil.

Provenance & Evidence