HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-chloro-1-methyl-4-nitro-1H-pyrazole → 4-(1-methyl-4-nitro-1H-pyrazol-5-yl)-1,4-diazepan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-chloro-1-methyl-4-nitro-1H-pyrazole | HCID 12344836 | — |
| Reactant | 1,4-Diazepan-2-one | HCID 13428532 | — |
| Product | 4-(1-methyl-4-nitro-1H-pyrazol-5-yl)-1,4-diazepan-2-one | HCID 58464860 | 92% |
Reaction Steps
Reaction of 5-chloro-1-methyl-4-nitro-1H-pyrazole and 1,4-diazepan-2-one gave 4-(1-methyl-4-nitro-1H-pyrazol-5-yl)-1,4-diazepan-2-one as an off-white solid (0.27 g, 92%). 1H NMR (400 MHz, CDCl3) δ 8.02 (s, 1H), 6.10 (s, 1H), 3.95-3.86 (m, 2H), 3.80 (s, 3H), 3.51-3.44 (m, 2H), 3.43-3.37 (m, 2H), 2.04-1.97 (m, 2H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08669361B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-e007fa00cbc84617abbcb3f2cc5cfbff |
| Source note | uspto-grants-2014_03 |