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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1185480Generated: November 2, 2026

HCID 68600866, compound → HCID 68600726, compound

https://huagongshe.com/reaction/1185480

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68600866HCID 68600866—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 68600726HCID 68600726—

Reaction Steps

To a solution of 1.4 g 3-Benzyloxycarbonylamino-azetidine-1-carboxylic acid butyl ester in 50 ml ethyl acetate were added 150 mg Pd/C (10%) and the suspension stirred under an atmosphere of hydrogen (1 bar) for 5 h. The reaction mixture was filtrated over a plug of Celite®, washed with ethyl acetate and concentrated. Yield: 740 mg colorless solid

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08669266B2
Source datasetuspto-grants-2014_03
ORD IDord-775500c5367e4fc0af6b7a9d14b6f0dc
Source noteuspto-grants-2014_03