HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1185748Generated: November 3, 2026
Thionyl Chloride → 6-Bromo-2-naphthoyl chloride
https://huagongshe.com/reaction/1185748
Participants
| Role | Name | HCID | Charge |
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| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-Bromo-2-naphthalenecarboxylic acid | HCID 4549852 | — |
| Product | 6-Bromo-2-naphthoyl chloride | HCID 21879606 | — |
Reaction Steps
6-Bromonaphthalene-2-carboxylic acid (25.1 g) was suspended in thionyl chloride (200 mL), stirred at 60° C. for 16 hours and evaporated under vacuum. Solid was dissolved in dichloromethane (50 mL) and evaporated under vacuum, giving 6-bromonaphthalene-2-carbonyl chloride (27.0 g, crude) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08669234B2 |
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| Source dataset | uspto-grants-2014_03 |
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| ORD ID | ord-1b25258842cf4adda33c1c96c67d73d7 |
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| Source note | uspto-grants-2014_03 |
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