HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1185964Generated: November 1, 2026
2-Mercaptoethanol → Hexadecyl 2-methylprop-2-enoate--octadecyl 2-methylprop-2-enoate (1/1)
https://huagongshe.com/reaction/1185964
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Mercaptoethanol | HCID 1567 | — |
| Reactant | Stearyl methacrylate | HCID 122600 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Hexadecyl 2-methylprop-2-enoate--octadecyl 2-methylprop-2-enoate (1/1) | HCID 169025 | — |
Reaction Steps
A monomer feed containing 55 g of hexadecylmethacrylate, 55 g octadecylmethacrylate, 68 g toluene, and 0.58 g 2-mercaptoethanol, and an initiator feed containing 40 g toluene and 1.65 g 2,2′-azobis-2-methylpropionitrile are slowly added to the reaction flask, using the separator funnels, over a period of two hours, with continuous agitation, while the temperature is maintained at reflux (110° C.), under a flow of nitrogen.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08671871B2 |
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| Source dataset | uspto-grants-2014_03 |
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| ORD ID | ord-8d97b1906ed54d90841311ccef7e7271 |
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| Source note | uspto-grants-2014_03 |
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