Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethylamine → (2S)-2-amino-5-(((tert-butoxy)carbonyl)amino)pentanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethylamine | HCID 8021 | — |
| 반응물 | Fmoc-Orn(Boc)-OH | HCID 2756114 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | (2S)-2-amino-5-(((tert-butoxy)carbonyl)amino)pentanoic acid | HCID 6993436 | 210% |
반응 단계
The compound obtained in Example 23-1 (250.8 mg) was dissolved in DMF (5 ml). After the addition of diethylamine. (0.5 ml), the mixture was stirred for 2 hours at room temperature. After the reaction, the solvent was removed by distillation under reduced pressure and the residue was dried under vacuum to obtain the title compound (269.1 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07098215B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-4dc70e910fce4c9ba040b32abaa97152 |
| 출처 메모 | uspto-grants-2006_08 |