Isopropylamine → 3-[Benzyl-(pyridine-3-sulfonyl)-amino]-N-isopropyl-benzamide

HRID 1186260Notes

Reaction equation

HRID 1186260 reaction equation
[CH2:1]([N:8]([S:18]([C:21]1[CH:22]=[N:23][CH:24]=[CH:25][CH:26]=1)(=[O:20])=[O:19])[C:9]1[CH:10]=[C:11]([CH:15]=[CH:16][CH:17]=1)[C:12]([OH:14])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:27]([NH2:30])([CH3:29])[CH3:28]>>[CH2:1]([N:8]([S:18]([C:21]1[CH:22]=[N:23][CH:24]=[CH:25][CH:26]=1)(=[O:19])=[O:20])[C:9]1[CH:10]=[C:11]([CH:15]=[CH:16][CH:17]=1)[C:12]([NH:30][CH:27]([CH3:29])[CH3:28])=[O:14])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 673107893-[Benzyl-(pyridine-3-sulfonyl)-amino]-benzoic acid

Product 1

HCID 461825043-[Benzyl-(pyridine-3-sulfonyl)-amino]-N-isopropyl-benzamide

Procedure

3-[Benzyl-(pyridine-3-sulfonyl)-amino]-N-isopropyl-benzamide was prepared from 3-[benzyl-(pyridine-3-sulfonyl)-amino]-benzoic acid and isopropylamine according to the method described for Example 2. HPLC retention time 5.46 min. Mass spectrum (APCI+) m/z 410 (M+H).

Sources & evidence

ORD record
ord-aceeecd9c1a7457e99da808be8cbfdaa
Source dataset
uspto-grants-2014_03
Patent number
US08673901B2

Reaction notes

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