HRID1186396

反应详情

EQUATION

反应方程式

HRID 1186396 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

According to Step 2 of Reference Example 8-65, by use of ethyl 3-(pyridin-3-yl)-2-butenoate (350 mg, 1.8 mmol) obtained in Step 1 of Reference Example 8-66, ethanol (4 mL) and 10% palladium carbon (70 mg), the mixture was stirred and reacted under a hydrogen atmosphere at room temperature for 2 hours. Thus, ethyl 3-(pyridin-3-yl)butanoate (339 mg, yield: 96%) was obtained.

WORKUP

后处理

  1. customreacted under a hydrogen atmosphere at room temperature for 2 hours