HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-amino-N-(2-methylphenyl)benzene-1-sulfonamide → 4-Amino-N-(4-methoxyphenyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-amino-N-(2-methylphenyl)benzene-1-sulfonamide | HCID 593569 | — |
| Reactant | N-(4-methoxyphenyl)-4-nitrobenzenesulfonamide | HCID 750280 | — |
| Product | 4-Amino-N-(4-methoxyphenyl)benzenesulfonamide | HCID 578975 | 79% |
Reaction Steps
(RK1-1-27E II) I This compound was prepared according to the procedure described for compound 12a except using 11g to obtain the required product as a light yellow solid, (197 mg, 79%). Mp: not determined; 1H NMR. (400 MHz, CDCl3) δ 7.45 (d, J=9.0 Hz, 2H), 6.96 (d, J=8.8 Hz, 2H), 6.76 (d, J=9.0 Hz, 2H), 6.58 (d, J=8.8 Hz, 2H), 6.09 (br s, 1H), 4.07 (br s, 2H), 3.76 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673910B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-7c000ce7d046416babd55b82c41da160 |
| Source note | uspto-grants-2014_03 |