HRID1186648

反应详情

EQUATION

反应方程式

HRID 1186648 的结构方程式

PROCEDURE

实验过程

(RK1-1-39) I This compound was prepared according to the procedure described for compound 12a except using 11h to obtain the required product as an orange-brown solid in (169 mg, 66%). Mp: not determined; 1H NMR (400 MHz, CDCl3) δ 7.50 (d, J=8.4 Hz, 1H), 6.99 (t, J=7.8 Hz, 1H), 6.82 (br s, 1H), 6.79-6.73 (m, 2H), 6.65 (br s, 1H), 6.11 (d, J=2.0 Hz, 1H), 6.09 (s, 1H), 3.99 (br s, 2H), 3.86 (s, 3H), 2.18 (s, 3H).

WORKUP

后处理

  1. custom(RK1-1-39) I This compound was prepared